Record Display for the EPA National Library Catalog

RECORD NUMBER: 85 OF 122

Main Title Protocol for the field validation of emission concentrations from stationary sources.
CORP Author Environmental Protection Agency, Research Triangle Park, NC. Office of Air Quality Planning and Standards.
Publisher U.S. Environmental Protection Agency,
Year Published 1991
Report Number EPA/450-4-90-015
Stock Number PB91-216184
OCLC Number 24230581
Subjects Air quality management
Additional Subjects Air pollution detection ; Statistical analysis ; Validation ; Field tests ; Emission factors ; Air pollution monitoring ; Stationary sources ; Precision
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=2000NDXT.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EKBD  EPA-450/4-90-015 Research Triangle Park Library/RTP, NC 10/05/1991
ELBD ARCHIVE EPA 450-4-90-015 Received from HQ AWBERC Library/Cincinnati,OH 10/04/2023
ESAD  EPA 450-4-90-015 Region 10 Library/Seattle,WA 03/23/2010
NTIS  PB91-216184 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 39 pages
Abstract
The purpose of the validation protocol is to determine bias and precision of the test method at the level of concentration in the gas stream. Procedures involve (1) introducing known concentrations of an analyte or comparing the method against a validated test method to determine bias and (2) using multiple sampling trains to determine precision. The protocol lists a number of important requirements for the validation of the test method. They include; use of EPA audit material; documenting and reporting results; procedures for determining bias and precision by means of isotopic and analyte spiking of multiple train samples or comparison to validated methods; and, procedures for calculating precision, bias and correction factors. The protocol also defines the acceptance criteria in terms of percent bias and precision and how the determined precision dictates future testing with the validated method.
Notes
"Office of Air Quality Planning and Standards, Technical Support Division." "Atmospheric Research and Exposure Assessment Laboratory, Quality Assurance Division." "EPA/450-4-90-015." "April 1991."