| Main Title |
Standardization of stationary source method for vinyl chloride / |
| Author |
Scheil, George W.
|
| CORP Author |
Midwest Research Inst., Kansas City, Mo.;Environmental Monitoring and Support Lab., Research Triangle Park, N.C. |
| Publisher |
Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory ; For sale by the National Technical Information Service, |
| Year Published |
1977 |
| Report Number |
EPA/600-4-77-026; EPA-68-02-1098 |
| Stock Number |
PB-271 513 |
| OCLC Number |
03854082 |
| ISBN |
pbk. |
| Subjects |
Vinyl chloride
|
| Additional Subjects |
Vinyl chloride ;
Quality assurance ;
Gas analysis ;
Air pollution ;
Industrial wastes ;
Combustion products ;
Field tests ;
Performance evaluation ;
Samples ;
Incinerators ;
Chemical analysis ;
Laboratory equipment ;
EPA method 106 ;
Air pollution detection ;
Stationary sources ;
Monomers
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| EKBD |
EPA-600/4-77-026 |
|
Research Triangle Park Library/RTP, NC |
07/25/2003 |
| ELBD ARCHIVE |
EPA 600-4-77-026 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| ELBD ARCHIVE |
EPA 600-4-77-026 |
|
AWBERC Library/Cincinnati,OH |
01/27/2022 |
| ESAD |
EPA 600-4-77-026 |
|
Region 10 Library/Seattle,WA |
03/23/2010 |
| NTIS |
PB-271 513 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
x, 40 pages : illustrations ; 28 cm. |
| Abstract |
A program was conducted to evaluate the proposed EPA Method 106 - Determination of Vinyl Chloride from Stationary Sources. Vinyl Chloride samples in Tedlar bags remain stable for more than one week. Aluminized Mylar bags can also be used if the samples are analyzed within two days. Several compounds can interfere with the gas chromatographic analysis by forming a single unresolved peak with vinyl chloride. Acetaldehyde and ethylene oxide are serious interferences with methanol and isobutane interfering under some conditions. Retention indices have been measured for several compounds on three useful GC columns. Nearly all samples can be satisfactorily resolved with the proper choice of column. Pressurized gas cylinders of vinyl chloride in nitrogen were used for calibrations. The cylinders were standardized against gravimetrically calibrated vinyl chloride permeation tubes. Field tests were also made at a polyvinyl chloride plant and a vinyl chloride monomer plant. No serious problems with the method were found in the field tests. |
| Notes |
Contract 68-02-1098. "May 1977." "EPA/600-4-77-026." |
