| Main Title |
Method development for determination of polychlorinated hydrocarbons in municipal sludge / |
| Author |
Rodriguez, Charles F., ;
McMahon, William A. ;
Thomas, Richard E.
|
| Other Authors |
|
| CORP Author |
Southwest Research Inst., San Antonio, TX.;Municipal Environmental Research Lab., Cincinnati, OH. |
| Publisher |
Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory and Municipal Environmental Research Laboratory, For sale by the National Technical Information Service. |
| Year Published |
1980 |
| Report Number |
EPA-600/2-80-029; EPA-68-03-2606 |
| Stock Number |
PB80-198401 |
| OCLC Number |
06575473 |
| ISBN |
pbk. |
| Subjects |
Hydrocarbons--Biodegradation ;
Pesticides--Biodegradation--United States ;
Sewage sludge ;
Water--Purification ;
Water Purification--(DNLM)D018508 ;
Pesticides--United States--Biodegradation
|
| Additional Subjects |
Pesticides ;
Chemical analysis ;
Extraction ;
Centrifuging ;
Chlorine organic compounds ;
Gas chromatography ;
Mass spectroscopy ;
Polychlorinated biphenyls ;
Sewage sludge
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| EHAM |
TD767.4.M37 |
|
Region 1 Library/Boston,MA |
04/29/2016 |
| EJBD |
EPA 600-2-80-029 |
|
Headquarters Library/Washington,DC |
08/31/2016 |
| EKBD |
EPA-600/2-80-029 |
|
Research Triangle Park Library/RTP, NC |
07/04/2003 |
| EKCD |
EPA-600/2-80-029 |
|
CEMM/GEMMD Library/Gulf Breeze,FL |
05/29/2018 |
| ELBD ARCHIVE |
EPA 600-2-80-029 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| EMBD |
EPA/600/2-80/029 |
|
NRMRL/GWERD Library/Ada,OK |
02/17/1995 |
| ERAD |
EPA 600/2-80-029 |
|
Region 9 Library/San Francisco,CA |
10/01/2012 |
| NTIS |
PB80-198401 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
vi, 65 pages : illustrations ; 28 cm. |
| Abstract |
The method provides a procedure for analysis of pesticides and PCB's in municipal sludge. The method includes extraction by a centrifuge technique of the chlorinated compounds from the sludge matrix; clean-up of the extract to remove interferences by sulfur precipitation as mercury sulfide, and by gel permeation of florisil chromatography; quantitation of the chlorinated compounds by an electron capture detector with GC chromatrography; and confirmation of the chlorinated compounds by GC/MS/computer. The method provides confirmation of single component pesticides at 0/3 mg of pesticide per Kg of sludges. The recommended extracting solvent is 15% methylene chloride, 2% acetone and 83% hexane. |
| Notes |
Issued Mar. 1980. Prepared by Southwest Research Institute, under contract no. Contract Number: 68-03-2606. |
