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RECORD NUMBER: 50 OF 69

Main Title Optimization of High-Speed GC/TOFMS for Method TO-14 Analysis.
Author Berkley, R. E. ; Akard, M. L. ; Gardner, B. D. ; Oliver, K. D. ; Jacumin, H. H. ;
CORP Author Environmental Protection Agency, Research Triangle Park, NC. ;ManTech Environmental Technology, Inc., Research Triangle Park, NC.
Publisher 2003
Year Published 2003
Stock Number PB2004-100890
Additional Subjects Air pollution detection ; Gas chromatography ; Mass spectrometry ; Organic compounds ; Chemical analysis ; Toxic substances ; Air pollution sampling ; Calibrations ; Canisters ; Vapors ; Performance ; Optimization ;
Holdings
Library Call Number Additional Info Location Last
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Status
NTIS  PB2004-100890 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 10p
Abstract
A fast gas chromatography/mass spectrometry (GC/MS) system (FGCMS) consisting of a high-speed gas chromatograph equipped with a narrow bandwidth injection accessory and a time-of-flight mass spectrometer detector is being optimized for analysis of Method TO-14 target compounds. The system consists entirely of commercially-available components. Turn-around time between sample injections has been reduced to six minutes, in contrast to an hour for conventional Method TO-14. Instrument configuration, control, and date processing procedures under development are described.