Record Display for the EPA National Library Catalog

RECORD NUMBER: 101 OF 295

Main Title Evaluation of sensitized fluorescence for polynuclear aromatic hydrocarbon detection /
Author Smith, T. R.
CORP Author TRW Defense and Space Systems Group, Redondo Beach, CA.;Industrial Environmental Research Lab., Research Triangle Park, NC.
Publisher U.S. Environmental Protection Agency, Industrial Environmental Research Laboratory ; National Information Service [distributor,
Year Published 1979
Report Number EPA-600/7-79-207; EPA-68-02-2689
Stock Number PB80-108475
OCLC Number 08372137
Subjects Fluorescence, Sensitized ; Polycyclic compounds ; Fluorescence, Sensitized ; Polycyclic compounds
Additional Subjects Aromatic polycyclic hydrocarbons ; Gas analysis ; Fluorescence ; Spot tests ; Chemical analysis ; Samples ; Combustion products ; Industrial wastes ; Performance evaluation ; Gas chromatography ; Mass spectroscopy ; Air pollution detection
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=9101FTXV.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EJBD  EPA 600-7-79-207 Headquarters Library/Washington,DC 03/31/2016
EKBD  EPA-600/7-79-207 Research Triangle Park Library/RTP, NC 01/02/2004
ELBD ARCHIVE EPA 600-7-79-207 Received from HQ AWBERC Library/Cincinnati,OH 10/04/2023
NTIS  PB80-108475 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation vi, 41 p. : ill. ; 28 cm.
Abstract
The report gives results of an evaluation of a fluorescent spot test for detecting the presence of polynuclear aromatic hydrocarbons (PAHs) as a screening technique for samples to be analyzed by Gas Chromatography/Mass Spectrometry (GC/MS). The test is based on the phenomenon of sensitized fluorescence and is capable of easily detecting 100 picograms of PAH in a 1 microliter sample, a level of sensitivity adequate for screening combustion effluent samples. Two interferences were observed: highly colored samples require dilution to allow viewing of the fluorescence level, and samples containing substantial amounts of phthalate esters produce false positive results. No false negative results were observed in the study. The test is adequate for screening combustion effluent samples prior to GC/MS analysis.
Notes
"TRW Defense and Space Systems Group." "August 1979." Includes bibliographical references. "Contract no. 68-02-2689, T.D. 104, program element no. INE624."