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Main Title

Measurement of Carbonyl Compounds from Stationary Source Emissions by a PFBHA-GC-ECD Method.

Author

Fan, Z. H. ; Peterson, M. R. ; Jayanty, R. K. M. ; Wilshire, F. W. ;

CORP Author

Research Triangle Inst., Research Triangle Park, NC.;Environmental Protection Agency, Research Triangle Park, NC. Office of Research and Development.

Publisher

18 Mar 98

Year Published

1998

Report Number

EPA-R-823866-01; EPA/600/A-98/049;

Stock Number

PB98-135643

Additional Subjects

Carbonyl compounds ; Air pollution sampling ; Gas chromatography ; Electron capture ; Stationary pollutant sources ; Air pollution sources ; Test methods ; Air pollution detection ; Emissions ; Chemical analysis ; Collecting methods ; PFBHA(Pentafluorobenzyl Hydroxylamine Hydrochloride)

Internet Access

Description	Access URL
	https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=P100U0I3.PDF

Holdings

Library	Call Number	Additional Info	Location	Last Modified	Checkout Status
NTIS	PB98-135643	Some EPA libraries have a fiche copy filed under the call number shown.		07/26/2022

Collation

18p

Abstract

This paper presents a study in the development of a test method for the measurement of carbonyls from stationary source emissions. This method involves collection of carbonyls in midget impingers, derivatization of carbonyls with O-2,3,4,5,6-pentafluorobenzyl hydroxylamine hydrochloride (PFBHA), separation of carbonyl-PFBHA derivatives by gas chromatography (GC), and measurement of the derivatives with electron capture detection (ECD). Formaldehyde, acetaldehyde, acrolein, acetone, butyraldehyde, methyl ethyl ketone, methyl isobutyl ketone, and hexaldehyde were selected as candidate for the method evaluation.

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