Record Display for the EPA National Library Catalog

RECORD NUMBER: 35 OF 48

OLS Field Name OLS Field Data
Main Title Method development for determination of polychlorinated hydrocarbons in municipal sludge /
Author Rodriguez, Charles F. ; McMahon, William A. ; Thomas, Richard E.
Other Authors
Author Title of a Work
McMahon, William A.,
Thomas, R. E.
CORP Author Southwest Research Inst., San Antonio, TX.;Municipal Environmental Research Lab., Cincinnati, OH.
Publisher Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory and Municipal Environmental Research Laboratory ; For sale by the National Technical Information Service,
Year Published 1980
Report Number EPA-600/2-80-029; EPA-68-03-2606
Stock Number PB80-198401
OCLC Number 06575473
ISBN pbk.
Subjects Hydrocarbons--Biodegradation. ; Pesticides--Biodegradation--United States. ; Sewage sludge. ; Water--Purification. ; Pesticides--United States--Biodegradation
Additional Subjects Pesticides ; Chemical analysis ; Extraction ; Centrifuging ; Chlorine organic compounds ; Gas chromatography ; Mass spectroscopy ; Polychlorinated biphenyls ; Sewage sludge
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=30000AUE.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EHAM  TD767.4.M37 Region 1 Library/Boston,MA 04/29/2016
EJBD ARCHIVE EPA 600-2-80-029 Headquarters Library/Washington,DC 08/19/2016
EJBD  EPA 600-2-80-029 Headquarters Library/Washington,DC 08/31/2016
EKBD  EPA-600/2-80-029 Research Triangle Park Library/RTP, NC 07/04/2003
EKCD  EPA-600/2-80-029 CEMM/GEMMD Library/Gulf Breeze,FL 05/29/2018
EMBD  EPA/600/2-80/029 NRMRL/GWERD Library/Ada,OK 02/17/1995
ERAD  EPA 600/2-80-029 Region 9 Library/San Francisco,CA 10/01/2012
NTIS  PB80-198401 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. 01/01/1988
Collation vi, 65 pages : illustrations ; 28 cm.
Abstract
The method provides a procedure for analysis of pesticides and PCB's in municipal sludge. The method includes extraction by a centrifuge technique of the chlorinated compounds from the sludge matrix; clean-up of the extract to remove interferences by sulfur precipitation as mercury sulfide, and by gel permeation of florisil chromatography; quantitation of the chlorinated compounds by an electron capture detector with GC chromatrography; and confirmation of the chlorinated compounds by GC/MS/computer. The method provides confirmation of single component pesticides at 0/3 mg of pesticide per Kg of sludges. The recommended extracting solvent is 15% methylene chloride, 2% acetone and 83% hexane.
Notes
Prepared by Southwest Research Institute, under contract no. 68-03-2606. Issued Mar. 1980.