Record Display for the EPA National Library Catalog


Main Title A one step method for the determination of carbamate pesticides by derivatization with [alpha]-bromo-2,3,4,5,6-pentafluorotoluene /
Author Jackson, Merrill D. ; Soileau, Stephen D. ; Sovocool, G. Wayne ; Sachleben, Richard A.
Other Authors
Author Title of a Work
Soileau, Stephen David,
Sovocool, G. Wayne.
Sachleben, Richard A.
CORP Author Health Effects Research Lab., Research Triangle Park, NC. Analytical Chemistry Branch.
Publisher Health Effects Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency,
Year Published 1979
Report Number EPA-600/4-79-077; EPA-600/4-79-036 [printing error - use 077]
Stock Number PB80-142847
OCLC Number 34707162
Additional Subjects Pesticides ; Carbamates ; Chemical analysis ; Trace elements ; Hydrolysis ; Bromine organic compounds ; Gas chromatography ; Toluene/bromo-pentafluoro ; Procedures
Internet Access
Description Access URL
Library Call Number Additional Info Location Last
EJBD ARCHIVE EPA 600-4-79-077 Headquarters Library/Washington,DC 01/04/2010
EJBD  EPA 600-4-79-077 Headquarters Library/Washington,DC 03/22/2016
EKBD  EPA-600/4-79-077 Research Triangle Park Library/RTP, NC 05/10/1996
EKCD  EPA-600/4-79-077 CEMM/GEMMD Library/Gulf Breeze,FL 07/25/2018
EMBD  EPA/600/4-79/077 NRMRL/GWERD Library/Ada,OK 05/24/1996
ESAD  EPA 600-4-79-077 Region 10 Library/Seattle,WA 03/23/2010
NTIS  PB80-142847 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation vii, 95 pages : illustrations ; 28 cm.
A procedure was developed for the determination of trace quantities of a broad range of carbamate pesticides. The carbamates were hydrolyzed and derivatized in a single step, using alkali and alpha-bromo-2,3,4,5,6-pentafluorotoluene (PFBB), and were subsequently analyzed using electron capture gas chromatography. This one step derivatization method created a novel derivative in which one fluorine on the PFB ring was displaced by an ethoxide ion via aromatic nucleophilic substitution.
"By Merrill D. Jackson, Stephen D. Soileau, G. Wayne Sovocool and Richard A. Sachleben, Environmental Toxicology Division, Health Effects Research Laboratory." Document no. changed after publication to EPA-600/4-79-077. No. EPA-600/4-79-036 belongs to title "Hydraulics of the Atchafalaya basin ..." (OCLC #5397078). "September 1979." Includes bibliographical references (pages 20-22).