Main Title |
A one step method for the determination of carbamate pesticides by derivatization with [alpha]-bromo-2,3,4,5,6-pentafluorotoluene / |
Author |
Jackson, Merrill D. ;
Soileau, Stephen D. ;
Sovocool, G. Wayne ;
Sachleben, Richard A.
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Other Authors |
|
CORP Author |
Health Effects Research Lab., Research Triangle Park, NC. Analytical Chemistry Branch. |
Publisher |
Health Effects Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency, |
Year Published |
1979 |
Report Number |
EPA-600/4-79-077; EPA-600/4-79-036 [printing error - use 077] |
Stock Number |
PB80-142847 |
OCLC Number |
34707162 |
Additional Subjects |
Pesticides ;
Carbamates ;
Chemical analysis ;
Trace elements ;
Hydrolysis ;
Bromine organic compounds ;
Gas chromatography ;
Toluene/bromo-pentafluoro ;
Procedures
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Internet Access |
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Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
EJBD |
EPA 600-4-79-077 |
|
Headquarters Library/Washington,DC |
03/22/2016 |
EKBD |
EPA-600/4-79-077 |
|
Research Triangle Park Library/RTP, NC |
05/10/1996 |
EKCD |
EPA-600/4-79-077 |
|
CEMM/GEMMD Library/Gulf Breeze,FL |
07/25/2018 |
ELBD ARCHIVE |
EPA 600-4-79-077 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
EMBD |
EPA/600/4-79/077 |
|
NRMRL/GWERD Library/Ada,OK |
05/24/1996 |
ESAD |
EPA 600-4-79-077 |
|
Region 10 Library/Seattle,WA |
03/23/2010 |
NTIS |
PB80-142847 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
vii, 95 pages : illustrations ; 28 cm. |
Abstract |
A procedure was developed for the determination of trace quantities of a broad range of carbamate pesticides. The carbamates were hydrolyzed and derivatized in a single step, using alkali and alpha-bromo-2,3,4,5,6-pentafluorotoluene (PFBB), and were subsequently analyzed using electron capture gas chromatography. This one step derivatization method created a novel derivative in which one fluorine on the PFB ring was displaced by an ethoxide ion via aromatic nucleophilic substitution. |
Notes |
"By Merrill D. Jackson, Stephen D. Soileau, G. Wayne Sovocool and Richard A. Sachleben, Environmental Toxicology Division, Health Effects Research Laboratory." Document no. changed after publication to EPA-600/4-79-077. No. EPA-600/4-79-036 belongs to title "Hydraulics of the Atchafalaya basin ..." (OCLC #5397078). "September 1979." Includes bibliographical references (pages 20-22). |