Main Title |
Field Evaluation of EPA Proposed Method 0040 (Sampling and Analysis of Volatile Organic Compounds Using Tedlar (Trade Name) Bags). |
Author |
McGaughey, J. F. ;
Bursey, J. T. ;
Merrill, R. G. ;
Fuerst, R. G. ;
Jackson, M. D. ;
|
CORP Author |
Eastern Research Group, Morrisville, NC.;Environmental Protection Agency, Research Triangle Park, NC. National Exposure Research Lab. |
Publisher |
1997 |
Year Published |
1997 |
Report Number |
EPA-68-D4-0022; EPA/600/A-97/069; |
Stock Number |
PB97-195432 |
Additional Subjects |
Air pollution sampling ;
Field tests ;
Test methods ;
Incinerators ;
Combustion products ;
Exhaust gases ;
Exhaust emissions ;
Air pollution sources ;
Stationary pollutant sources ;
Gas chromatography ;
Mass spectroscopy ;
Chemical analysis ;
Analytical methods ;
Performance evaluation ;
Statistical analysis ;
Volatile organic compounds ;
EPA Method 0040 ;
VOST(Volatile Organic Sampling Train)
|
Internet Access |
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
NTIS |
PB97-195432 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
9p |
Abstract |
A field test has been performed to evaluate EPA Proposed Method 0040 (Sampling of Principal Organic Hazardous Constituents from Combustion Sources Using Tedlar Bags), a method for the collection of volatile organic compounds above the range of EPA Method 0030 (VOST). In the laboratory studies, a design for the sampling train was developed and the train was evaluated using dynamic spiking techniques. An analytical methodology using gas chromatography/mass spectrometry (GC/MS) was also developed. A field test of the methodology was performed to determine the systematic error (bias) and random error (precision) under stationary source sampling conditions. Four similar trains were operated using a quadruplicate sampling probe, with dynamic spiking of two trains with volatile organic compounds, while sampling emissions from a coal combustion source. Analytical data were statistically evaluated according EPA Method 301. Fifteen of eighteen volatile organic test compounds met Method 301 acceptance criteria for performance. |