Main Title |
Determination of diphenylamine in industrial and municipal wastewaters |
Author |
Warner, J. S. ;
Engel, T. M. ;
Mondron, P. J.
|
Other Authors |
|
CORP Author |
Battelle Columbus Labs., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH. |
Publisher |
U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, |
Year Published |
1985 |
Report Number |
EPA-600/4-85-025; EPA-68-03-2956; PB85190874 |
Stock Number |
PB85-190874 |
OCLC Number |
20848412 |
Subjects |
Chemical analysis ;
Industrial wastes ;
Pesticides ;
Gas chromatography ;
Extraction ;
Water analyses ;
Water pollution ;
Concentration(Composition) ;
Anilines ;
Water pollution detection ;
Municipal wastes ;
Publicly owned wastewater treatment ;
Diphenylamine ;
CAS 122-39-4
|
Additional Subjects |
Chemical analysis ;
Industrial wastes ;
Pesticides ;
Gas chromatography ;
Extraction ;
Water analyses ;
Water pollution ;
Concentration(Composition) ;
Anilines ;
Water pollution detection ;
Municipal wastes ;
Publicly owned wastewater treatment ;
Diphenylamine ;
CAS 122-39-4
|
Internet Access |
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
EJBD ARCHIVE |
EPA 600-4-85-025 |
|
Headquarters Library/Washington,DC |
02/10/2011 |
EJBD |
EPA 600/4-85-025 |
|
Headquarters Library/Washington,DC |
02/28/2007 |
NTIS |
PB85-190874 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
vi, 38 p. : ill. ; 28 cm. |
Abstract |
A method was developed for the determination of diphenylamine in wastewaters. The method development program consisted of a literature review: determination of extraction efficiency for each compound from water using methylene chloride; development of a deactivated silica gel cleanup procedure; and determination of suitable gas chromatographic (GC) analysis conditions. The final method was applied to Columbus POTW secondary effluent in order to determine the precision and accuracy of the method. The method detection limit (MDL) for diphenylamine in distilled water was 1.6 microgram/l. In wastewaters it may be higher due to interfering compounds. |
Notes |
Cover title. Project officer: Thomas Pressley. "EMSL number 468-M." "Method 620." "EPA/600/4-85/025." "...Contract No. 68-03-2956 by Battelle Columbus Laboratories...." |