| Main Title |
Standard Operating Procedure for the Laboratory Analysis of Lead in Paint, Bulk Dust, and Soil by Ultrasonic, Acid Digestion and Inductively Coupled Plasma Emission Spectrometric Measurement. |
| Author |
Grohse, P. M. ;
Gutknecht, W. F. ;
Luk, K. K. ;
Wilson, B. M. ;
Van Hise, C. C. ;
|
| CORP Author |
Research Triangle Inst., Research Triangle Park, NC. Center for Environmental Measurements and Quality Assurance.;Environmental Protection Agency, Research Triangle Park, NC. National Exposure Research Lab. |
| Publisher |
Sep 97 |
| Year Published |
1997 |
| Report Number |
EPA-68-D1-0009 ;EPA-68-D5-0040; EPA/600/R-95/111; |
| Stock Number |
PB98-136963 |
| Additional Subjects |
Lead(Metal) ;
Chemical analysis ;
Laboratory tests ;
Paints ;
Dust ;
Soils ;
Lead compojnds ;
Ultrasonic tests ;
Sampling ;
Sample preparation ;
Laboratory procedures ;
Ultrasonic testing ;
Quality control ;
Standard operating procedures ;
Acid digestion ;
Inductively couples plasma emission spectroscopy ;
RSD(Relative Standard Deviation)
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB98-136963 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
48p |
| Abstract |
The details and performance of a simplified extraction procedure and analysis for three media are provided. Paint, bulk dust, and soil are collected using standard or referenced methods. Up to 0.25 g of paint, bulk dust, or soil weighted out and placed in a 50-mL centrifuge tube. Five mL of 25% (v/v) nitric acid is added and the sample is ultrasonicated for 30 minutes. |
