Record Display for the EPA National Library CatalogRECORD NUMBER: 1 OF 12
|Main Title||Analytical Methods for a National Study of Chemical Residues in Fish. 1. Polychlorinated Dibenzo-p-dioxins/Dibenzofurans.|
|Author||Marquis, P. J. ; Hackett, M. ; Holland, L. G. ; Larsen, M. L. ; Butterworth, B. ;|
|CORP Author||Environmental Research Lab.-Duluth, MN. ;Wisconsin Univ.-Superior. Center for Lake Superior Environmental Studies.|
|Additional Subjects||Fishes ; Water pollution effects(Animals) ; Dioxin ; Furans ; Test methods ; Analytical chemistry ; Quality assurance ; Chemical analysis ; Tables(Data) ; Chlorohydrocarbons ; Bioaccumulation ; Chromatography ; Mass spectroscopy ; Reprints ; PCDD(Polychlorinated dibenzo-p-dioxins) ; Polychlorinated dibenzo-p-dioxin ; PCDFs(Polychlorinated dibenzofurans) ; Polychlorinated dibenzofurans ; Chemical residues ; National Bioaccumulation Study ; Xenobiotics|
Analytical Methods were developed to determine the concentration of polychlorinated dibenzo-p-dioxin/polychlorinated dibenzofuran (PCDD/PCDF) in fish tissue for a national survey conducted by the U.S. Environmental Protection Agency (EPA). The method was designed to achieve a relatively low cost per sample while maintaining adequate quality control. It utilizes a Soxhlet extraction, acid-celite, florisil and carbon-silica gel chromatography, and HRGC/HRMS analysis. The minimum level of detection for 2,3,7,8-TCDD is approximately 1 pg/g. Rigorous quality assurance/quality control criteria have been developed to assure the validity of the data.