| Main Title |
Standardization of method 11 at a petroleum refinery / |
| Author |
Scheil, George W. ;
Sharp., Michael C.
|
| Other Authors |
|
| CORP Author |
Midwest Research Inst., Kansas City, Mo.;Environmental Monitoring and Support Lab., Research Triangle Park, N.C. |
| Publisher |
U.S. Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory, |
| Year Published |
1977 |
| Report Number |
EPA/600-4-77-008a; EPA/600-4-77-008b; EPA-68-02-1098 |
| Stock Number |
PB-266 886 |
| OCLC Number |
52753212 |
| Additional Subjects |
Petroleum industry ;
Refineries ;
Gas analysis ;
Hydrogen sulfide ;
Field tests ;
Chemical analysis ;
Laboratory equipment ;
Air pollution ;
Sampling ;
Standards ;
Thiols ;
Industrial wastes ;
Combustion products ;
Procedures ;
Stationary sources ;
Air pollution detection ;
EPA method 11
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| EJBD |
EPA 600-4-77-008a |
c.1 |
Headquarters Library/Washington,DC |
03/26/2014 |
| EJBD |
EPA 600-4-77-008b |
c.1 |
Headquarters Library/Washington,DC |
03/26/2014 |
| EKBD |
EPA-600/4-77-008a |
v.1 |
Research Triangle Park Library/RTP, NC |
05/16/2023 |
| EKBD |
EPA-600/4-77-008a,b |
|
Research Triangle Park Library/RTP, NC |
08/01/2003 |
| EKBD |
EPA-600/4-77-008b |
v.2 |
Research Triangle Park Library/RTP, NC |
05/16/2023 |
| ELBD ARCHIVE |
EPA 600-4-77-008a |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| ELBD RPS |
EPA 600-4-77-008a |
v.1, repository |
AWBERC Library/Cincinnati,OH |
02/20/2018 |
| ELBD ARCHIVE |
EPA 600-4-77-008b |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| ELBD RPS |
EPA 600-4-77-008b |
v.2, repository |
AWBERC Library/Cincinnati,OH |
02/20/2018 |
| ESAD |
EPA 600-4-77-008a,b |
|
Region 10 Library/Seattle,WA |
09/05/2017 |
| NTIS |
PB-266 886 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
2 volumes : illustrations ; 28 cm |
| Abstract |
Method 11 (Federal Register, 39, pp. 9321-9323, March 8, 1974), 'Determination of Hydrogen Sulfide Emissions from Stationary Sources,' is subject to serious mercaptan interference. Several alternate absorbing reagents were evaluated, including several salts of cadmium and zinc. The solution pH was adjusted to obtain a high collection efficiency for H2S without also collecting mercaptans. The most selective absorbing solution was 0.16 M cadmium sulfate at a pH of 3.0. The H2S collection efficiency was 96 percent, and mercaptan concentration equal to the H2S gave results about 5 percent high. The effect of 14 variables on the analysis were evaluated in a ruggedness test. The optimized procedure was then field tested at three refineries under a variety of conditions. The laboratory and field tests were then used to write a final version of the procedure. |
| Notes |
Project Officer: M. Rodney Midgett. "EPA/600-4-77-008a." "January 1977." "EPA/600-4-77-008b." Midwest Research Institute Contract Number: 68-02-1098 "EPA-600/4-77-008a"--Cover "EPA-600/4-77-008b"--Cover |
