Main Title |
Identification and analysis of polychlorinated biphenyls and other related chemicals in municipal sewage sludge samples / |
Author |
Erickson, Mitchell D. ;
Pellizzari., Edo D.
|
Other Authors |
|
CORP Author |
Research Triangle Inst., Research Triangle Park, N.C.;Environmental Protection Agency, Washington, D.C. Office of Toxic Substances. |
Publisher |
Research Triangle Institute, |
Year Published |
1977 |
Report Number |
68-01-1978; EPA 560/6-77-021; EPA-68-01-1978; EPA 560/1977 RTI/001 |
Stock Number |
PB-273 192 |
OCLC Number |
43256423 |
Subjects |
Organochlorine compounds ;
Polychlorinated biphenyls ;
Sewage sludge--Analysis ;
Chemical compounds ;
Polychlorinated biphenyls (PCBs)
|
Additional Subjects |
United States--Toxic Substances Control Act ;
Chemical analysis ;
Sludge ;
Chlorine organic compounds ;
Samples ;
Extraction ;
Gas chromatography ;
Mass spectroscopy ;
Laboratory equipment ;
Sampling ;
Polychlorinated biphenyls ;
Sewage sludge ;
Polychlorinated naphthalenes ;
Polychlorinated aniline ;
Benzene/chloro ;
Produces ;
Sulfate/dimethyl
|
Internet Access |
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
EJBD |
TD767.4.R84 1977 |
|
Headquarters Library/Washington,DC |
08/21/2012 |
EJED |
EPA 560/6-77-021 |
|
OCSPP Chemical Library/Washington,DC |
01/14/2000 |
EJED |
EPA 560/1977 RTI/001 |
|
OCSPP Chemical Library/Washington,DC |
09/10/1999 |
EKBD |
EPA-560/6-77-021 |
|
Research Triangle Park Library/RTP, NC |
05/30/2003 |
ELBD ARCHIVE |
EPA 560-6-77-021 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
ESAD |
EPA 560-6-77-021 |
|
Region 10 Library/Seattle,WA |
08/28/2018 |
NTIS |
PB-273 192 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
xiv, 143 pages : illustrations, charts ; 28 cm |
Abstract |
Methods were developed for the extraction, clean-up and GC/MS analysis of polychlorinated biphenyls (PCBs) and related chemicals in municipal sludge samples. Each of the sludge samples received from nine major United States cities was processed to yield a neutral fraction and two acid fractions which were methylated with dimethylsulfate and diazomethane, respectively. Samples were cleaned up by silica gel column chromatography. A total of 35 chlorinated compounds were found in the full scan GC/MS analysis, including polychlorobiphenyls, polychloronaphthalenes, polychloroaniline, polychlorobenzene and DDE. Some chlorinated compounds remain unidentified. |
Notes |
"U.S. Environmental Protection Agency, Office of Toxic Substances." "EPA 7560/6-77-021." "Contract No. 68-01-1978." "August 1977." "Project Officer: Dr. Vincent J. DeCarlo." |