Record Display for the EPA National Library CatalogRECORD NUMBER: 7 OF 19
|Main Title||Determination of Pentachlorophenol in Blood, Urine, Tissue, and Clothing.|
|Author||Barthel, W. F. ; Curley, August ; Thrasher, C. L. ; Sedlak, V. A. ; Armstrong., Robert ;|
|CORP Author||National Communicable Disease Center, Atlanta, Ga.|
|Stock Number||PB-276 899, PB-276 897|
|Additional Subjects||Chemical analysis ; Chlorine organic compounds ; Blood analysis ; Urine ; Tissues(Biology) ; Clothing ; Electron capture ; Gas chromatography ; Mass spectroscopy ; Thin layer chromatography ; Fungus resistant coatings ; Reprints ; Phenol/pentachloro ; Electron capture gas chromatography|
An epidemic with two deaths occurred in a nursery in St. Louis after the use of pentachlorophenol as a mildew preventive with the laundry detergent. Samples of blood, urine, tissue, and clothing from the nursery were extracted with ethyl ether. The ether solution was extracted with 5% sodium hydroxide; the basic solution was acidified and then extracted with benzene. The benzene solution was analyzed by electron capture gas chromatography, using a 3% diethylene glycol succinate column with 2% sirupy phosphoric acid on 60-80 mesh Chromosorb G. Pentachlorophenol was found in the samples in sufficient quantity to account for the epidemic. The presence of pentachlorophenol was confirmed by gas chromatography-mass spectroscopy and by thin layer analysis.
found in PB-276 897 titled: Journal articles on pesticide chemical analysis. Group 5.