| Main Title |
Analytical procedures for aniline and selected derivatives in wastewater and sludge / |
| Author |
Riggin, Ralph M. ;
Lucas, S. V. ;
Cole, T. F. ;
Birts, M. A.
|
| Other Authors |
|
| CORP Author |
Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH. |
| Publisher |
U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, |
| Year Published |
1984 |
| Report Number |
EPA/600/4-84/009; EPA-68-03-2952 |
| Stock Number |
PB84-140102 |
| Subjects |
Lucas, SV
|
| Additional Subjects |
Chemical analysis ;
Waste water ;
Water pollution ;
Industrial wastes ;
Gas chromatography ;
Measuring instruments ;
Mass spectroscopy ;
Sludge ;
Extraction ;
Sewage sludge ;
Water pollution detection ;
High performance liquid chromatography ;
EPA method 625 ;
Solid wastes
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB84-140102 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
231 pages ; 28 cm |
| Abstract |
This study involved the development and validation of analytical methods for determining aniline and 18 halogen and nitro-substituted derivatives in industrial wastewater and municipal sludge. Gas chromatography (GC) with a nitrogen-phosphorus detector (NPD) was found to be well suited as a determinative technique for anilines in wastewater. Detection limits of 1-5 micrograms/L were achieved using both packed and capillary columns. A GC-MS approach which was essentially the same as U.S. EPA Method 625 was found to be useful for identifying and determining anilines in industrial wastewater at the low micrograms/L level. A U.S. EPA Interim Method developed by EMSL-Cincinnati for the determination of priority pollutants in municipal sludge was evaluated and optimized for the determination of anilines. Detection limits of 50-300 micrograms/kg were achieved. |
| Notes |
Caption title. "January 1984." "EPA-600/4-84-007." Microfiche. |
