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Mixing with microwaves: solvent-free and catalyst-free synthesis of pyrazoles and diazepines
Citation:
Reddy, B., R. Varma, AND J. Leazer. Mixing with microwaves: solvent-free and catalyst-free synthesis of pyrazoles and diazepines. TETRAHEDRON LETTERS. Elsevier Science Ltd, New York, NY, 54(12):1538-1541, (2013).
Impact/Purpose:
submitted for publication in the Royal Society of Chemistry (RSC) journal, Green Chemistry
Description:
A simple and facile condensation of hydrazines/hydrazides and diamines with 1,3-diketones/β-ketoester leads to the preparation of pyrazoles and diazepines in high yields. This eco-friendly protocol is accelerated by microwave heating and efficiently carried out without any reaction solvent or catalyst in as little as five minutes.
URLs/Downloads:
PYRAZOLES AND DIAZEPINES - MANUSCRIPT.PDF (PDF, NA pp, 159.191 KB, about PDF)http://www.sciencedirect.com/science/article/pii/S0040403913000658
Record Details:
Record Type:DOCUMENT( JOURNAL/ PEER REVIEWED JOURNAL)
Product Published Date:03/04/2013
Record Last Revised:03/04/2013
OMB Category:Other
Record ID:
252835