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One-pot Catalyst-free Synthesis of β- and γ-Hydroxy Sulfides Using Diaryliodonium Salts and Microwaves

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Citation:

Reddy, B., R. Varma, AND J. Leazer. One-pot Catalyst-free Synthesis of β- and γ-Hydroxy Sulfides Using Diaryliodonium Salts and Microwaves. European Journal of Organic Chemistry. Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, Germany, 2012(35):6852-6855, (2012).

Impact/Purpose:

for publication in the Royal Society of Chemistry (RSC) Journal, Chemical Communications

Description:

A facile one-pot high-yield protocol is described for the preparation of β- and γ-hydroxy sulfides directly from diaryliodonium salts, potassium thiocyanate, and ethane-1,2-diol (ethylene glycol)/propane-1,3-diol (β-propylene glycol) without the need for any additional catalyst or base or solvent.

Record Details:

Record Type:DOCUMENT( JOURNAL/ PEER REVIEWED JOURNAL)
Record Released:01/09/2013
Record Last Revised:01/09/2013
OMB Category:Other
Record ID: 248753