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Citation:

Arizona Border Study Consortium. U.S.-MEXICO BORDER PROGRAM ARIZONA BORDER STUDY--STANDARD OPERATING PROCEDURE FOR OPERATION, CALIBRATION, AND MAINTENANCE OF THE PERKIN-ELMER ZEEMAN/5000 SYSTEM ATOMIC ABSORPTION SPECTROPHOTOMETER (BCO-L-6.0). U.S. Environmental Protection Agency, Washington, D.C.

Description:

The purpose of this SOP is to outline the start-up, calibration, operation, and maintenance procedures for the Perkin-Elmer 5000 atomic absorption spectrophotometer (PE 5000 AA), and the Perkin Elmer 5000 Zeeman graphite furnace atomic absorption spectrophotometer (PE 5000Z GFAA). These procedures are used for the determination of the trace target metals As, Ba, Cd, Cr, Cu, Mn, Ni, Pb, Se, V, and Zn in soil, house dust, filter, and surface and dermal wipe sample digestates. This procedure was followed to ensure consistent data retrieval during the Arizona NHEXAS project and the Border study. Keywords: laboratory; FAA; GFAA; metals.

The U.S.-Mexico Border Program is sponsored by the Environmental Health Workgroup of the Border 2012 Program. The Environmental Health Workgroup's mission is "to identify and address, in a binational framework, environmental factors that pose the highest risk to human health so that exposure to such factors may be reduced." To accomplish this mission, studies are performed to help understand the interrelationships between environmental conditions and human health. The Arizona Border Study, sponsored by the Environmental Health Workgroup, is an extension of the Arizona National Human Exposure Assessment Survey (NHEXAS) Phase I Study. The Arizona Border Study collected household environmental and personal samples for chemical analysis, and questionnaires were administered. The NHEXAS Phase I Questionnaires were used with some adjustments and were organized into seven modules (Descriptive, Baseline, Technician, Follow-up, Time and activity diary, Dietary diary, and Supplement) for simplicity in administration. The questionnaires are designed for collecting information that can be temporally related to the exposure, concentration, and/or biological measurements. The Arizona Border study sampled residences determined by a population-based probability research design for populations in the Arizona counties bordering Mexico, and measured metals, pesticides, polynuclear aromatic hydrocarbons (PAHs), and volatile organic compounds (VOCs). Analytical results were obtained under strict QA/QC requirements during collection, processing, and final deposition into databases. In addition, strict standard operating procedures were followed throughout the Arizona Border study. The study was conducted by a consortium composed of the University of Arizona, Battelle Columbus, and the Illinois Institute of Technology. Data collection occurred between September 1997 and July 1998 for the participating households.

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