OLS : Record


Main Title Identification and analysis of polychlorinated biphenyls and other related chemicals in municipal sewage sludge samples /
Author Erickson, Mitchell D.; Pellizzari., Edo D.
CORP Author Research Triangle Inst., Research Triangle Park, N.C.;Environmental Protection Agency, Washington, D.C. Office of Toxic Substances.
Publisher Research Triangle Institute,
Place Published Research Triangle Park, NC
Year Published 1977
Report Number 68-01-1978; EPA 560/6-77-021; EPA-68-01-1978; EPA 560/1977 RTI/001
Stock Number PB-273 192
OCLC Number 43256423
Subjects United States.--Toxic Substances Control Act.; Chemical analysis; Sludge; Chlorine organic compounds; Samples; Extraction; Gas chromatography; Mass spectroscopy; Laboratory equipment; Sampling; Polychlorinated biphenyls; Sewage sludge; Polychlorinated naphthalenes; Polychlorinated aniline; Benzene/chloro; Produces; Sulfate/dimethyl
Subject Added Ent Organochlorine compounds.; Polychlorinated biphenyls.; Sewage sludge--Analysis.; Chemical compounds; Polychlorinated biphenyls (PCBs)
Internet Access
Description Access URL
Library   Call Number Additional Info Location Date Modified
EIAD EPA 560/6-77-021 Region 2 Library/New York,NY 06/27/2003
EJBD ARCHIVE EPA 560-6-77-021 Headquarters Library/Washington,DC 09/05/2012
EJBD TD767.4.R84 1977 Headquarters Library/Washington,DC 08/21/2012
EJED EPA 560/6-77-021 OCSPP Chemical Library/Washington,DC 01/14/2000
EJED EPA 560/1977 RTI/001 OCSPP Chemical Library/Washington,DC 09/10/1999
EKBD EPA-560/6-77-021 Research Triangle Park Library/RTP, NC 05/30/2003
EOAD EPA 560/6-77-021 Region 8 Technical Library/Denver,CO 11/18/2005
NTIS PB-273 192 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Collation xiv, 143 p. : ill., charts ; 28 cm.
Abstract Methods were developed for the extraction, clean-up and GC/MS analysis of polychlorinated biphenyls (PCBs) and related chemicals in municipal sludge samples. Each of the sludge samples received from nine major United States cities was processed to yield a neutral fraction and two acid fractions which were methylated with dimethylsulfate and diazomethane, respectively. Samples were cleaned up by silica gel column chromatography. A total of 35 chlorinated compounds were found in the full scan GC/MS analysis, including polychlorobiphenyls, polychloronaphthalenes, polychloroaniline, polychlorobenzene and DDE. Some chlorinated compounds remain unidentified.
Notes "U.S. Environmental Protection Agency, Office of Toxic Substances." "EPA 7560/6-77-021." "Contract No. 68-01-1978." "August 1977." "Project Officer: Dr. Vincent J. DeCarlo."
Author Added Ent
Erickson, Mitchell D.;
Pellizzarri, E. D.;
DeCarlo, Vincent J.
Corporate Au Added Ent United States. Environmental Protection Agency. Office of Toxic Substances.; Research Triangle Institute.
PUB Date Free Form 1977
NTIS Prices PC A08/MF A01
BIB Level m
OCLC TAG 19s 42306357
OCLC Time Stamp 20120823104437
Cataloging Source OCLC/T
Language eng
Origin OCLC
OCLC Rec Leader 01555cam 2200397Ia 45020