OLS : Record

RECORD NUMBER: 32 OF 45

Main Title Analytical procedures for aniline and selected derivatives in wastewater and sludge {microform} /
Author Riggin, Ralph M.; Lucas, S. V.; Cole, T. F.; Birts, M. A.
CORP Author Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.
Publisher U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory,
Place Published Cincinnati, OH :
Year Published 1984
Report Number EPA/600/4-84/009; EPA-68-03-2952
Stock Number PB84-140102
OCLC Number 48593111
Subjects Chemical analysis; Waste water; Water pollution; Industrial wastes; Gas chromatography; Measuring instruments; Mass spectroscopy; Sludge; Extraction; Sewage sludge; Water pollution detection; High performance liquid chromatography; EPA method 625; Solid wastes
Subject Added Ent Lucas, S. V
Holdings
Library   Call Number Additional Info Location Date Modified
ERBD PB84-140102 NERL/ESD-LV Library/Las Vegas,NV 12/14/2001
NTIS PB84-140102 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Collation 231 p. ; 28 cm.
Abstract This study involved the development and validation of analytical methods for determining aniline and 18 halogen and nitro-substituted derivatives in industrial wastewater and municipal sludge. Gas chromatography (GC) with a nitrogen-phosphorus detector (NPD) was found to be well suited as a determinative technique for anilines in wastewater. Detection limits of 1-5 micrograms/L were achieved using both packed and capillary columns. A GC-MS approach which was essentially the same as U.S. EPA Method 625 was found to be useful for identifying and determining anilines in industrial wastewater at the low micrograms/L level. A U.S. EPA Interim Method developed by EMSL-Cincinnati for the determination of priority pollutants in municipal sludge was evaluated and optimized for the determination of anilines. Detection limits of 50-300 micrograms/kg were achieved.
Notes Caption title. "January 1984." "EPA-600/4-84-007." Microfiche.
Author Added Ent
Cole, T. F.;
Birts, M. A.
Corporate Au Added Ent Environmental Monitoring and Support Laboratory. ; Battelle Columbus Division (Ohio).
PUB Date Free Form 1984.
NTIS Prices PC A11/MF A01
BIB Level m
OCLC Time Stamp 20011213183946
Cataloging Source OCLC/T
Language eng
Origin OCLC
Type MERGE
OCLC Rec Leader 01109cam 2200289Ka 45170