OLS : Record

RECORD NUMBER: 32 OF 45

Main Title

Analytical procedures for aniline and selected derivatives in wastewater and sludge {microform} /

Author

Riggin, Ralph M.; Lucas, S. V.; Cole, T. F.; Birts, M. A.

CORP Author

Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.

Publisher

U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory,

Place Published

Cincinnati, OH :

Year Published

1984

Report Number

EPA/600/4-84/009; EPA-68-03-2952

Stock Number

PB84-140102

OCLC Number

48593111

Subjects

Chemical analysis; Waste water; Water pollution; Industrial wastes; Gas chromatography; Measuring instruments; Mass spectroscopy; Sludge; Extraction; Sewage sludge; Water pollution detection; High performance liquid chromatography; EPA method 625; Solid wastes

Subject Added Ent

Lucas, S. V

Holdings

Library		Call Number	Additional Info	Location	Date Modified
ERBD		PB84-140102		NERL/ESD-LV Library/Las Vegas,NV	12/14/2001
NTIS		PB84-140102	Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy.	NTIS	01/01/1988

Collation

231 p. ; 28 cm.

Abstract

This study involved the development and validation of analytical methods for determining aniline and 18 halogen and nitro-substituted derivatives in industrial wastewater and municipal sludge. Gas chromatography (GC) with a nitrogen-phosphorus detector (NPD) was found to be well suited as a determinative technique for anilines in wastewater. Detection limits of 1-5 micrograms/L were achieved using both packed and capillary columns. A GC-MS approach which was essentially the same as U.S. EPA Method 625 was found to be useful for identifying and determining anilines in industrial wastewater at the low micrograms/L level. A U.S. EPA Interim Method developed by EMSL-Cincinnati for the determination of priority pollutants in municipal sludge was evaluated and optimized for the determination of anilines. Detection limits of 50-300 micrograms/kg were achieved.

Notes

Caption title. "January 1984." "EPA-600/4-84-007." Microfiche.

Author Added Ent

Cole, T. F.;

Birts, M. A.

Corporate Au Added Ent

Environmental Monitoring and Support Laboratory. ; Battelle Columbus Division (Ohio).

PUB Date Free Form

1984.

NTIS Prices

PC A11/MF A01

BIB Level

OCLC Time Stamp

20011213183946

Cataloging Source

OCLC/T

Language

eng

Origin

OCLC

Type

MERGE

OCLC Rec Leader

01109cam 2200289Ka 45170

OLS : Record

RECORD NUMBER: 32 OF 45

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