OLS : Record

RECORD NUMBER: 6 OF 563

Main Title

A one step method for the determination of carbamate pesticides by derivatization with [alpha]-bromo-2,3,4,5,6-pentafluorotoluene /

Author

Jackson, Merrill D.; Soileau, Stephen D.; Sovocool, G. Wayne; Sachleben, Richard A.

CORP Author

Health Effects Research Lab., Research Triangle Park, NC. Analytical Chemistry Branch.

Publisher

Health Effects Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency,

Place Published

Research Triangle Park, N.C.

Year Published

1979

Report Number

EPA-600/4-79-077; EPA-600/4-79-036 [printing error - use 077]

Stock Number

PB80-142847

OCLC Number

34707162

Subjects

Pesticides; Carbamates; Chemical analysis; Trace elements; Hydrolysis; Bromine organic compounds; Gas chromatography; Toluene/bromo-pentafluoro; Procedures

Internet Access

Description	Access URL
	http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=20012V9M.txt
	http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=2000HVQR.txt

Holdings

Library		Call Number	Additional Info	Location	Date Modified
EIAD		EPA-600/4-79-077		Region 2 Library/New York,NY	04/21/2006
EJAD		EPA 600/4-79-036		Region 3 Library/Philadelphia, PA	01/28/2000
EJBD	ARCHIVE	EPA 600-4-79-077		Headquarters Library/Washington,DC	01/04/2010
EKAM		EPA-600/4-79-077		Region 4 Library/Atlanta,GA	03/28/1998
EKBD		EPA-600/4-79-077		Research Triangle Park Library/RTP, NC	05/10/1996
EMBD		EPA/600/4-79/077		GWERD Library/Ada,OK	05/24/1996
EOAD		EPA 600/4-79-077		Region 8 Technical Library/Denver,CO	03/21/2011
ESAD		EPA 600-4-79-077		Region 10 Library/Seattle,WA	03/23/2010
NTIS		PB80-142847	Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy.	NTIS	06/23/1988

Collation

vii, 95 p. : ill. ; 28 cm.

Abstract

A procedure was developed for the determination of trace quantities of a broad range of carbamate pesticides. The carbamates were hydrolyzed and derivatized in a single step, using alkali and alpha-bromo-2,3,4,5,6-pentafluorotoluene (PFBB), and were subsequently analyzed using electron capture gas chromatography. This one step derivatization method created a novel derivative in which one fluorine on the PFB ring was displaced by an ethoxide ion via aromatic nucleophilic substitution.

Notes

"By Merrill D. Jackson, Stephen D. Soileau, G. Wayne Sovocool and Richard A. Sachleben, Environmental Toxicology Division, Health Effects Research Laboratory." Document no. changed after publication to EPA-600/4-79-077. No. EPA-600/4-79-036 belongs to title "Hydraulics of the Atchafalaya basin ..." (OCLC #5397078). "September 1979." Includes bibliographical references (p. 20-22).

Author Added Ent

Soileau, Stephen David,;

Sovocool, G. Wayne.;

Sachleben, Richard A.

Corporate Au Added Ent

Health Effects Research Laboratory (Research Triangle Park, N.C.). Environmental Toxicology Division.; United States. Environmental Protection Agency. Office of Research and Development.

Title Ser Add Ent

Research reporting series. Environmental monitoring.

Alternate Title

One step method for the determination of carbamate pesticides by derivatization with alpha-bromo-2,3,4,5,6-pentafluorotoluene

NTIS Title Notes

Final rept..

PUB Date Free Form

Sep 79

Series Title Traced

Research reporting series.

Series Title Untraced

Research reporting series. 4, Environmental monitoring.

Category Codes

6F; 7D; 68E; 57P; 99A

NTIS Prices

PC A06/MF A01

Primary Description

600/11

BIB Level

Control Number

323775018

OCLC Time Stamp

20110307114242

Cataloging Source

OCLC/T

Language

eng

Origin

OCLC

Type

MERGE

OCLC Rec Leader

01917cam 2200349Ka 45020

OLS : Record

RECORD NUMBER: 6 OF 563

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