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RECORD NUMBER: 6 OF 562

Main Title A one step method for the determination of carbamate pesticides by derivatization with [alpha]-bromo-2,3,4,5,6-pentafluorotoluene /
Author Jackson, Merrill D.; Soileau, Stephen D.; Sovocool, G. Wayne; Sachleben, Richard A.
CORP Author Health Effects Research Lab., Research Triangle Park, NC. Analytical Chemistry Branch.
Publisher Health Effects Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency,
Place Published Research Triangle Park, N.C.
Year Published 1979
Report Number EPA-600/4-79-077; EPA-600/4-79-036 [printing error - use 077]
Stock Number PB80-142847
OCLC Number 34707162
Subjects Pesticides; Carbamates; Chemical analysis; Trace elements; Hydrolysis; Bromine organic compounds; Gas chromatography; Toluene/bromo-pentafluoro; Procedures
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=20012V9M.txt
http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=2000HVQR.txt
Holdings
Library   Call Number Additional Info Location Date Modified
EIAD EPA-600/4-79-077 Region 2 Library/New York,NY 04/21/2006
EJAD EPA 600/4-79-036 Region 3 Library/Philadelphia, PA 01/28/2000
EJBD ARCHIVE EPA 600-4-79-077 Headquarters Library/Washington,DC 01/04/2010
EKAM EPA-600/4-79-077 Region 4 Library/Atlanta,GA 03/28/1998
EKBD EPA-600/4-79-077 Research Triangle Park Library/RTP, NC 05/10/1996
EMBD EPA/600/4-79/077 GWERD Library/Ada,OK 05/24/1996
EOAD EPA 600/4-79-077 Region 8 Technical Library/Denver,CO 03/21/2011
ESAD EPA 600-4-79-077 Region 10 Library/Seattle,WA 03/23/2010
NTIS PB80-142847 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation vii, 95 p. : ill. ; 28 cm.
Abstract A procedure was developed for the determination of trace quantities of a broad range of carbamate pesticides. The carbamates were hydrolyzed and derivatized in a single step, using alkali and alpha-bromo-2,3,4,5,6-pentafluorotoluene (PFBB), and were subsequently analyzed using electron capture gas chromatography. This one step derivatization method created a novel derivative in which one fluorine on the PFB ring was displaced by an ethoxide ion via aromatic nucleophilic substitution.
Notes "By Merrill D. Jackson, Stephen D. Soileau, G. Wayne Sovocool and Richard A. Sachleben, Environmental Toxicology Division, Health Effects Research Laboratory." Document no. changed after publication to EPA-600/4-79-077. No. EPA-600/4-79-036 belongs to title "Hydraulics of the Atchafalaya basin ..." (OCLC #5397078). "September 1979." Includes bibliographical references (p. 20-22).
Author Added Ent
Soileau, Stephen David,;
Sovocool, G. Wayne.;
Sachleben, Richard A.
Corporate Au Added Ent Health Effects Research Laboratory (Research Triangle Park, N.C.). Environmental Toxicology Division.; United States. Environmental Protection Agency. Office of Research and Development.
Title Ser Add Ent Research reporting series. Environmental monitoring.
Alternate Title One step method for the determination of carbamate pesticides by derivatization with alpha-bromo-2,3,4,5,6-pentafluorotoluene
NTIS Title Notes Final rept..
PUB Date Free Form Sep 79
Series Title Traced Research reporting series.
Series Title Untraced Research reporting series. 4, Environmental monitoring.
Category Codes 6F; 7D; 68E; 57P; 99A
NTIS Prices PC A06/MF A01
Primary Description 600/11
BIB Level m
Control Number 323775018
OCLC Time Stamp 20110307114242
Cataloging Source OCLC/T
Language eng
Origin OCLC
Type MERGE
OCLC Rec Leader 01917cam 2200349Ka 45020