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RECORD NUMBER: 39 OF 82

Main Title Manual of analytical quality control for pesticides and related compounds in human and environmental samples : a compendium of systematic procedures designed to assist in the prevention and control of analytical problems /
Author Sherma, Joseph.; Beroza, Morton
CORP Author Health Effects Research Laboratory (Research Triangle Park, N.C.); Health Effects Research Laboratory (Research Triangle Park, N.C.). Environmental Toxicology Division.; Association of Official Analytical Chemists.
Publisher U.S. Environmental Protection Agency, Office of Research and Development, Health Effects Research Laboratory,
Place Published Research Triangle Park, N.C.
Year Published 1979
Report Number EPA-600/1-79-008; 68-02-2474; PB-298711; EPA-68-02-2474
Stock Number PB 298 711
OCLC Number 05052388
Subjects Pesticides--Analysis; Chemical analysis; Quality control; Manuals; Urine; Samples; Bioassay; Extraction; Standards; Residues; Animals; Blood chemical analysis; Naphthols; Adsorbents; Gas chromatography; Storage; Containers; Column packings; Herbicides; Carbamates; Food analysis; Tissues(Biology); Humans; Water pollution; Air pollution; Gas analysis; Water analysis; Sediments; Insecticides; Soil analysis; Plants(Botany); Separation; Spectrophotometry; Mass spectroscopy; Polarography; Calibrating; Metabolism; Sampling; Procedures; Standard reference materials; Thin layer chromatography; Phenol/nitro; Carbamic acid/N-methyl; Polychlorinated biphenyls; Urea/ethylene-thio; Nuclear magnetic resonance; Quality assurance; Visible spectrum; Fluorescence; Infrared spectroscopy
Subject Added Ent Pesticides--Analysis.
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=2000ARLJ.txt
Holdings
Library   Call Number Additional Info Location Date Modified
EJDD EPA-600/1-79-008 OASQA Library/Fort Meade,MD 03/26/1999
EJED EPA 600/1-79-008 OCSPP Chemical Library/Washington,DC 11/17/1989
EKAM EPA/600/1-79-008 Region 4 Library/Atlanta,GA 12/03/1999
EKBD EPA-600/1-79-008 Research Triangle Park Library/RTP, NC 09/07/2001
ELDD EPA-600/1-79-008 NHEERL/MED Library/Duluth,MN 08/14/1998
EMBD EPA/600/1-79/008 GWERD Library/Ada,OK 09/29/1995
EOAD EPA-600/1-79-008 Region 8 Technical Library/Denver,CO 03/18/2005
EOBD EPA 600/1-79-008 NEIC Library/Denver,CO 11/09/2009
ERBD EPA/600/1-79/008 NERL/ESD-LV Library/Las Vegas,NV 02/15/1997
NTIS PB-298 711 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Edition Rev. 1979.
Collation xi, 402 p. : ill. ; 28 cm.
Abstract This manual provides the pesticide chemist with a systematic protocol for the quality control of analytical procedures and the problems that arise in the analysis of human or environmental media. It also serves as a guide to the latest and most reliable methodology available for the analysis of pesticide residues in these and other sample matrices. The sections dealing with inter- and intra-laboratory quality control, the evaluation and standardization of materials used, and the operation of the gas chromatograph are intended to highlight and provide advice in dealing with many problems which constantly plague the pesticide analytical chemist. Many aspects of the problem areas involved in extraction and isolation techniques for pesticides in various types of samples are discussed. Techniques for confirming the presence or absence of pesticides in sample materials are treated at some length. This highly important area provides validation of data obtained by the more routine analytical procedures. The gas chromatograph, being the principal instrument currently used in pesticide analysis, often requires simple servicing or troubleshooting. A section addressing some of these problems is included. Last, but by no means least in importance, is a short dissertation of the value and need for systematic training programs for pesticide chemists.
Notes Cover title. "Environmental Toxicology Division, Health Effects Research Laboratory." "January 1979." Includes bibliographical references. "Contract no. 68-02-2474." "EPA-600/1-79-008."
Supplementary Notes Revision of report dated Feb 76, PB-261 019. Prepared in cooperation with Association of Official Analytical Chemists, Washington, DC.
Author Added Ent
Beroza, Morton,;
Watts, Randall R.;
Thompson, Jack F.
Corporate Au Added Ent Health Effects Research Laboratory (Research Triangle Park, N.C.); Health Effects Research Laboratory (Research Triangle Park, N.C.). Environmental Toxicology Division.; Association of Official Analytical Chemists.
PUB Date Free Form 1979
NTIS Prices PC A18/MF A01
BIB Level m
Document Type BC
OCLC Time Stamp 20091104172952
Cataloging Source OCLC/T
Language eng
SUDOCS Number EP 1.8:P 43/4/979
Origin OCLC
Type CAT
OCLC Rec Leader 02031cam 2200469Ia 45020


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