OLS : Record


Main Title A method for the sampling and analysis of polychlorinated biphenyls (PCBs) in ambient air /
Author Stratton, Charles L.
Publisher Quality Assurance Branch, Environmental Monitoring and Support Laboratory, Office of Research and Development, U.S. Environmental Protection Agency ; Office of Toxic Substances, U.S. Environmental Protection Agency,
Place Published Research Triangle Park, N.C. Washington, D.C.
Year Published 1978
Report Number EPA 600-4-78-048; 68-01-2978; EPA-68-01-2978
Stock Number PB-288 410
OCLC Number 38134505
Subjects Gas analysis; Chlorine organic compounds; Chemical analysis; Sampling; Air pollution; Concentration(Composition); Field tests; Gas chromatography; Polychlorinated biphenyls; Air pollution detection; Biphenyl/perchloro; Aroclor 1016; Aroclor 1242; Procedures
Subject Added Ent Polychlorinated biphenyls--Analysis.
Internet Access
Description Access URL
Library   Call Number Additional Info Location Date Modified
EIAD EPA 600-4-78-048 Region 2 Library/New York,NY 12/03/2004
EJBD ARCHIVE EPA 600-4-78-048 Headquarters Library/Washington,DC 05/07/2012
EJBD EPA 600-4-78-048 c.1 Headquarters Library/Washington,DC 11/04/2013
EJED EPA 600/4-78-048 OCSPP Chemical Library/Washington,DC 08/25/2000
EKBD EPA-600-4-78-048 Research Triangle Park Library/RTP, NC 09/02/2014
ELDD EPA-600/4-78-048 NHEERL/MED Library/Duluth,MN 08/25/2000
ERAD EPA 600/4-78-048 Region 9 Library/San Francisco,CA 10/29/2012
ESAD EPA 600-4-78-048 Region 10 Library/Seattle,WA 01/02/1998
NTIS PB-288 410 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Collation x, 106, 27 p. : ill. ; 28 cm.
Abstract A method was developed for the sampling and analysis of polychlorinated biphenyls (PCBs) in air. An easily constructed, high-volume sampling system is employed with porous polyurethane foam as the collection medium. The sample is collected at the rate of 0.6 to 1.0 cu m per minute. Laboratory procedures described in this document permit the quantitative analysis of even the most volatile PCB species in an air sample. A perchlorination technique for the quantitative analysis of PCB has been adapted for use. The technique is shown to convert even the most volatile PCB species to decachlorobiphenyl for simple and direct quantitative analysis. Data is presented to show conversion efficiencies of a variety of PCBs to decachlorobiphenyl of 101 + or - 6 percent over the range of 0.103 to 10.0 micrograms. A ruggedness test was conducted which indicates the proposed perchlorination technique can yield reliable interlaboratory results. The perchlorination technique is generally necessary for the analysis of low (i.e., less than 25 ng/cu m airborne levels of PCB. The analytical method is effective for the analysis of airborne PCB levels within at least the range of 1 ng/cu m to 50 micrograms/cu m. (Portions of this document are not fully legible)
Notes "EPA 600/4-78/048." EPA contract no. 68-01-2978. Includes bibliographical references.
Author Added Ent
Whitlock, Stuart A.;
Allan, J. Mark.
Corporate Au Added Ent Environmental Monitoring and Support Laboratory (Research Triangle Institute). Quality Assurance Branch.; United States. Environmental Protection Agency. Office of Toxic Substances.
Title Ser Add Ent Environmental monitoring series.
PUB Date Free Form 1978
Series Title Traced Environmental monitoring series
Series Title Untraced Environmental monitoring series
NTIS Prices PC A07/MF A01
BIB Level m
OCLC Time Stamp 20140827100934
Cataloging Source OCLC/T
Language eng
Origin OCLC
OCLC Rec Leader 01605cam 2200349Ka 45020